An in situ EDXRD kinetic and mechanistic study of the hydrothermal crystallization of TiO2 nanoparticles from nitric acid peptized sol

An in situ EDXRD kinetic and mechanistic study of the hydrothermal crystallization of TiO2 nanoparticles from nitric acid peptized sol–gel

Published:2015 Issue:9 Volume:17 Page:2013-2020
ISSN:1466-8033
Container-title:CrystEngComm
language:en
Short-container-title:CrystEngComm

Author:

Rehan Mohammad¹²³⁴⁵,Kale Girish M.⁶²³⁴,Lai Xiaojun¹²³⁴

Affiliation:

1. Institute of Particle Science and Engineering (IPSE)

2. School of Chemical and Process Engineering

3. University of Leeds

4. Leeds LS2 9JT, UK

5. Center of Excellence in Environmental Studies (CEES)

6. Institute for Materials Research (IMR)

Abstract

In situ EDXRD has been used to probe the reaction kinetics and mechanism of the hydrothermal crystallization of TiO₂ nanoparticles. The process was found to involve a diffusion-controlled mechanism based on the Avrami–Erofe'ev kinetic model.

Funder

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2015/CE/C4CE02270J

Reference57 articles.

1. Light-induced amphiphilic surfaces

2. Titanium dioxide based high temperature carbon monoxide selective sensor

3. High H2 sensing performance of anodically oxidized TiO2 film contacted with Pd

4. A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO2 films

5. Bactericidal and Detoxification Effects of TiO2 Thin Film Photocatalysts

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