Convenient two step synthesis of 29Si labelled tetraalkoxysilanes-Reference-Cited by-同舟云学术

Convenient two step synthesis of 29Si labelled tetraalkoxysilanes

Published:2020 Issue:88 Volume:56 Page:13631-13633
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Gericke Robert¹²³⁴⁵^ORCID,Gondek Christoph¹²³⁴⁵,Stapf André¹²³⁴⁵^ORCID,Wagler Jörg¹²³⁴⁵^ORCID,Kroke Edwin¹²³⁴⁵^ORCID,Brendler Erica¹²⁶⁴⁵^ORCID

Affiliation:

1. Technische Universität Bergakademie Freiberg

2. Department of Chemistry and Physics

3. Institute of Inorganic Chemistry

4. 09599 Freiberg

5. Germany

6. Institute of Analytical Chemistry

Abstract

Starting from silicon dioxide or silicon a scalable, reliable synthesis of ²⁹Si enriched tetraethoxysilane, an essential sol–gel precursor, is presented.

Funder

Deutsche Forschungsgemeinschaft

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2020/CC/D0CC05525E

Reference34 articles.

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5. Measurements of spin-lattice relaxation times, T1, in Na2O-MgO-SiO2 glasses doped with MnO