Solid-phase extraction followed by gas chromatography-mass spectrometry for the quantitative analysis of semi-volatile hydrocarbons in hydraulic fracturing wastewaters

Author:

Regnery Julia123,Coday Bryan D.12345,Riley Stephanie M.123,Cath Tzahi Y.123

Affiliation:

1. Colorado School of Mines

2. Golden

3. USA

4. Carollo Engineers

5. Broomfield

Abstract

A versatile method was developed for the quantitative analysis of semi-volatile linear aliphatic hydrocarbons in the n-C10 to n-C32 range and 16 PAH in hydraulic fracturing wastewaters using C18 SPE followed by GC-MS.

Funder

U.S. Department of Energy

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Reference21 articles.

1. Chemical constituents and analytical approaches for hydraulic fracturing waters

2. Biocides in Hydraulic Fracturing Fluids: A Critical Review of Their Usage, Mobility, Degradation, and Toxicity

3. J. Kochany , PAHs in Natural Waters: Natural and Anthropogenic Sources, and Environmental Behaviour, in Wastewater Treatment: Occurrence and Fate of Polycyclic Aromatic Hydrocarbons, ed. A. J. Forsgren, CRC Press, Taylor & Francis Group, Boca Raton, FL, 2015

4. Characterization of hydraulic fracturing flowback water in Colorado: Implications for water treatment

5. Chemical Analysis of Wastewater from Unconventional Drilling Operations

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