Ethyl acetate as an acetyl source and solvent for acetylation of alcohols by KOH-Reference-Cited by-同舟云学术

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Ethyl acetate as an acetyl source and solvent for acetylation of alcohols by KOH

Published:2024 Issue:18 Volume:14 Page:12574-12579
ISSN:2046-2069
Container-title:RSC Advances
language:en
Short-container-title:RSC Adv.

Author:

Wang Xiaodan¹²,Sun Huilin¹²,Cheng Yao²,Yang Wenfei²,Wang Xinmei²,Xiong Liting²,Li Yiying³,Wang Jinhui¹²,Gan Chunli¹,Lin Chunguang²,Xu Huanjun²^ORCID

Affiliation:

1. Department of Medicinal Chemistry and Natural Medicine Chemistry, College of Pharmacy, Harbin Medical University, Harbin, 150081, China

2. School of Science, Qiongtai Normal University, Haikou 571127, China

3. College of Basic Medicine and Life Sciences, Hainan Medical University, Haikou, 571127, China

Abstract

A mild, efficient and convenient procedure for the acetylation of alcohols with EtOAc as acetyl source and solvent mediated by KOH was reported.

Funder

National Natural Science Foundation of China

Natural Science Foundation of Hainan Province

Hainan Association for Science and Technology

National Science and Technology Major Project

National College Students Innovation and Entrepreneurship Training Program

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/RA/D3RA08717D

Reference37 articles.

1. Investigation of new acyloxy derivatives of cholic acid and their esters as drug absorption modifiers

2. Straightforward and efficient synthesis of 3-benzyloxy-4-bromopicolinate ester and 3-benzyloxy-5-bromopicolinate ester, common building blocks for pharmaceuticals and agrochemicals

3. Transesterification

4. Palladium-Catalyzed Esterification of Carboxylic Acids with Aryl Iodides

5. Unprecedented acetylation of phenols using a catalytic amount of magnesium powder

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