Single step derivatization with CF3 enone of thiophene at ambient temperature to determine propellant grade hydrazines: a study by GC and GC-MS-Reference-Cited by-同舟云学术

Single step derivatization with CF3 enone of thiophene at ambient temperature to determine propellant grade hydrazines: a study by GC and GC-MS

Published:2015 Issue:1 Volume:140 Page:330-339
ISSN:0003-2654
Container-title:The Analyst
language:en
Short-container-title:Analyst

Author:

Subramanian Selvakumar¹²³⁴⁵,Narayanasastri Somanathan⁶⁷⁸⁹¹⁰,Kami Reddy Audisesha Reddy¹²³⁴⁵

Affiliation:

1. Chemical Testing Lab

2. Solid Propellant Space Booster Plant

3. SDSC-SHAR Centre

4. Indian Space Research Organization (ISRO)

5. Sriharikota 524124

6. Polymer Division

7. Central Leather Research Institute (CLRI)

8. Council of Scientific and Industrial Research (CSIR)

9. Chennai 600020

10. India

Abstract

A simple, highly selective and rapid gas chromatography method (packed column with flame ionization detection) has been developed to determine hydrazine and monomethylhydrazine individually and for selective determination of hydrazine in the UH 25 mixture in organic medium.

Publisher

Royal Society of Chemistry (RSC)

Subject

Electrochemistry,Spectroscopy,Environmental Chemistry,Biochemistry,Analytical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2015/AN/C4AN01648C

Reference44 articles.

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3. H. Yang , J.Wan, H.Shu, X.Liu, R. S.Lakshmanan, R.Guntupalli, W.Howard, J.Hu and B. A.Chin, Sensors Hand book, Mc Graw-Hill Publishing, New York, 2009, vol. 38, p. 761

4. H. W. Schiessl and I. K.Othmer, Encyclopedia of Chemical Technology, Wiley publishers, New York, 3rd edn, 1980

5. S. Selvakumar , N.Sridharan and K.Audisesha Reddy, Report on analysis of carbon dioxide in Hydrazine by GC method - ISRO- SHAR-01-R-TR-054-2006

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