Long-chain mercury carboxylates relevant to saponification in oil and tempera paintings: XRPD and ssNMR complementary study of their crystal structures-Reference-Cited by-同舟云学术

Long-chain mercury carboxylates relevant to saponification in oil and tempera paintings: XRPD and ssNMR complementary study of their crystal structures

Published:2022 Issue:10 Volume:51 Page:4019-4032
ISSN:1477-9226
Container-title:Dalton Transactions
language:en
Short-container-title:Dalton Trans.

Author:

Barannikov Ruslan¹²^ORCID,Kočí Eva¹,Bezdička Petr¹,Kobera Libor³^ORCID,Mahun Andrii³⁴,Rohlíček Jan⁵,Plocek Jiří¹,Švarcová Silvie¹^ORCID

Affiliation:

1. Institute of Inorganic Chemistry of the Czech Academy of Sciences, ALMA Laboratory, Husinec-Řež 1001, 250 68 Husinec-Řež, Czech Republic

2. Department of Inorganic Chemistry, Faculty of Science, Charles University in Prague, Hlavova 2030/8, 128 43 Prague 2, Czech Republic

3. Institute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovského nám. 2, 162 06 Praha 6, Czech Republic

4. Department of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, 128 40, Prague 2, Czech Republic

5. Institute of Physics of the Czech Academy of Sciences, Na Slovance 1999/2, 182 21 Praha 8, Czech Republic

Abstract

Mercury palmitate, stearate and palmitate-stearates were synthesized and characterized by ssNMR, XRPD, IR and DSC to provide reference materials for the identification of saponification-related degradation products in paintings.

Funder

Akademie Věd České Republiky

Ministerstvo Školství, Mládeže a Tělovýchovy

Grantová Agentura České Republiky

Publisher

Royal Society of Chemistry (RSC)

Subject

Inorganic Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2022/DT/D1DT04160F

Reference58 articles.

1. Mixed lead carboxylates relevant to soap formation in oil and tempera paintings: the study of the crystal structure by complementary XRPD and ssNMR