SDPD-SX: combining a single crystal X-ray diffraction setup with advanced powder data structure determination for use in early stage drug discovery-Reference-Cited by-同舟云学术

SDPD-SX: combining a single crystal X-ray diffraction setup with advanced powder data structure determination for use in early stage drug discovery

Published:2022 Issue:24 Volume:24 Page:4337-4340
ISSN:1466-8033
Container-title:CrystEngComm
language:en
Short-container-title:CrystEngComm

Author:

Kabova Elena A.¹^ORCID,Blundell Charles D.²^ORCID,Muryn Christopher A.³,Whitehead George F. S.³^ORCID,Vitorica-Yrezabal Inigo J.³^ORCID,Ross Marta J.¹^ORCID,Shankland Kenneth¹^ORCID

Affiliation:

1. School of Chemistry, Food and Pharmacy, University of Reading, Whiteknights, Reading, Berks RG6 6AD, UK

2. C4X Discovery, Manchester One, 53 Portland Street, Greater Manchester, M1 3LD, UK

3. Department of Chemistry, The University of Manchester, Oxford Road, Manchester M13 9PL, UK

Abstract

A method for routine molecular crystal structure determination on very small (typically <0.1 mg) amounts of crystalline material using powder X-ray diffraction data from a laboratory-based single-crystal diffractometer is reported.

Publisher

Royal Society of Chemistry (RSC)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2022/CE/D2CE00387B

Reference20 articles.

1. X-ray diffractometry for the structure determination of a submicrometre single powder grain

2. SFX analysis of non-biological polycrystalline samples

3. Chemical crystallography by serial femtosecond X-ray diffraction

4. X-Ray Diffraction from Magnetically Oriented Microcrystal Suspension

5. Single-crystal structure determination from microcrystalline powders (∼5 μm) by an orientation attachment mountable on an in-house X-ray diffractometer

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