Radical annulation of a designed diene system: access to nitro-benzo[<i>b</i>]azepines-Reference-Cited by-同舟云学术

Radical annulation of a designed diene system: access to nitro-benzo[b]azepines

Published:2022 Issue:69 Volume:58 Page:9658-9661
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Sun Kai¹^ORCID,Zhang Yan¹,Tian Miao¹,Wang Zhichuan¹,Zhao Dongyang¹,Wang Shilong¹,Tang Shi²^ORCID,Zhang Zhen¹^ORCID

Affiliation:

1. College of Chemistry and Chemical Engineering, Yantai University, Yantai, 264005, Shandong, P. R. China

2. College of Chemistry and Chemical Engineering, Jishou University, Jishou, 416000, China

Abstract

A O2N˙-triggered addition 7-endo cyclization to nitro-benzo[b]azepines is reported with good chemo- and regioselectivity. Large-scale operation and handy N-Ts and N-Cbz deprotection reveal the utility of this methodology.

Funder

National Natural Science Foundation of China

Natural Science Foundation of Shandong Province

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2022/CC/D2CC02688K

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