Synthesis, protonation equilibrium and peculiar thermal decomposition behavior of cyclo-tri-μ-imidotetraphosphate

Author:

Maki Hideshi1234,Ryousi Kazuomi1234,Nariai Hiroyuki1234,Mizuhata Minoru1234

Affiliation:

1. Department of Chemical Science and Engineering

2. Graduate School of Engineering

3. Kobe University

4. Kobe 657-8501, Japan

Abstract

The synthesis and isolation of the sodium salt ofcyclo-tri-μ-imidotetraphosphate,i.e.Na4cP4O9(NH)3·H2O, were achieved by the hydrolysis of Na4cP4O8(NH)4·2H2O under very weak acidic conditions,i.e.using 0.2 mol L−1propionic acid and the pH-controlled recrystallization procedure.

Publisher

Royal Society of Chemistry (RSC)

Subject

Inorganic Chemistry

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