Synthesis, protonation equilibrium and peculiar thermal decomposition behavior of cyclo-tri-μ-imidotetraphosphate-Reference-Cited by-同舟云学术

Synthesis, protonation equilibrium and peculiar thermal decomposition behavior of cyclo-tri-μ-imidotetraphosphate

Published:2014 Issue:30 Volume:43 Page:11611-11623
ISSN:1477-9226
Container-title:Dalton Trans.
language:en
Short-container-title:Dalton Trans.

Author:

Maki Hideshi¹²³⁴,Ryousi Kazuomi¹²³⁴,Nariai Hiroyuki¹²³⁴,Mizuhata Minoru¹²³⁴

Affiliation:

1. Department of Chemical Science and Engineering

2. Graduate School of Engineering

3. Kobe University

4. Kobe 657-8501, Japan

Abstract

The synthesis and isolation of the sodium salt ofcyclo-tri-μ-imidotetraphosphate,i.e.Na₄cP₄O₉(NH)₃·H₂O, were achieved by the hydrolysis of Na₄cP₄O₈(NH)₄·2H₂O under very weak acidic conditions,i.e.using 0.2 mol L⁻¹propionic acid and the pH-controlled recrystallization procedure.

Publisher

Royal Society of Chemistry (RSC)

Subject

Inorganic Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2014/DT/C4DT00601A

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