Synthesis of metal–organic frameworks by continuous flow

Author:

Bayliss Peter A.123,Ibarra Ilich A.12345,Pérez Eduardo123,Yang Sihai123,Tang Chiu C.678,Poliakoff Martyn123,Schröder Martin123

Affiliation:

1. School of Chemistry

2. University of Nottingham

3. University Park, UK

4. Instituto de Investigaciones en Materiales

5. Universidad Nacional Autónoma de México

6. Diamond Light Source

7. Harwell Science and Innovation Campus

8. Oxfordshire, UK

Abstract

MIL-53(Al) can be prepared via reaction in continuous flow in only 5–6 minutes with a space time yield of 1300 kg m−3 d−1. Extraction of free terephthalic acid from within the pores of MIL-53(Al) using supercritical ethanol has been developed.

Publisher

Royal Society of Chemistry (RSC)

Subject

Pollution,Environmental Chemistry

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