Concise total synthesis of (−)-berkelic acid <i>via</i> regioselective spiroacetal/pyran formation-Reference-Cited by-同舟云学术

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Concise total synthesis of (−)-berkelic acid via regioselective spiroacetal/pyran formation

Published:2024 Issue:24 Volume:60 Page:3331-3334
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Hanada Shogo¹²^ORCID,Yoshida Masahito¹³^ORCID,Kigoshi Hideo¹³⁴^ORCID

Affiliation:

1. Degree Programs in Pure and Applied Sciences, Graduate School of Science and Technology, Japan

2. Chemical & Biological Technology Labs., Astellas Pharma Inc., Miyukigaoka 21, Tsukuba, Ibaraki 305-8585, Japan

3. Department of Chemistry, Faculty of Pure and Applied Sciences, Japan

4. Alliance for the Research on the Mediterranean and North Africa (ARENA), University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8571, Japan

Abstract

Concise total synthesis of (−)-berkelic acid is accomplished through regioselective tandem spiroacetal/pyran formation of a simpler alkyne precursor.

Funder

Naito Foundation

Japan Society for the Promotion of Science

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/CC/D4CC00166D

Reference21 articles.

1. Berkelic Acid, A Novel Spiroketal with Selective Anticancer Activity from an Acid Mine Waste Fungal Extremophile

2. A Synthesis-Driven Structure Revision of Berkelic Acid Methyl Ester

3. Total Synthesis of Berkelic Acid

4. Biomimetic Synthesis of the Tetracyclic Core of Berkelic Acid

5. Synthesis of (−)-Berkelic Acid

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