Rapid acquisition of data dense solid-state CPMG NMR spectral sets using multi-dimensional statistical analysis-Reference-Cited by-同舟云学术

Rapid acquisition of data dense solid-state CPMG NMR spectral sets using multi-dimensional statistical analysis

Published:2018 Issue:26 Volume:20 Page:18082-18088
ISSN:1463-9076
Container-title:Physical Chemistry Chemical Physics
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Mason H. E.¹²³⁴^ORCID,Uribe E. C.⁵⁶³⁴,Shusterman J. A.⁷⁸⁹⁴

Affiliation:

1. Physical and Life Science Directorate

2. Lawrence Livermore National Laboratory

3. Livermore

4. USA

5. Systems Research and Analysis

6. Sandia National Laboratories

7. Department of Chemistry

8. Hunter College of City University of New York

9. New York

Abstract

Tensor-rank decomposition methods have been applied to variable contact time ²⁹Si{¹H} CP/CPMG NMR data sets to extract NMR dynamics information and dramatically decrease conventional NMR acquisition times.

Funder

Biological and Environmental Research

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2018/CP/C8CP02382D

Reference32 articles.

1. Spatial distribution of organic functional groups supported on mesoporous silica nanoparticles: a study by conventional and DNP-enhanced 29Si solid-state NMR

2. Mesoporous Silica Nanoparticles Loaded with Surfactant: Low Temperature Magic Angle Spinning 13C and 29Si NMR Enhanced by Dynamic Nuclear Polarization

3. Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials

4. One hundred fold overall sensitivity enhancements for Silicon-29 NMR spectroscopy of surfaces by dynamic nuclear polarization with CPMG acquisition

5. Surface-selective direct 17O DNP NMR of CeO2 nanoparticles

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