Monitoring off-resonance signals with SHARPER NMR – the MR-SHARPER experiment

Author:

Davy Matthew1ORCID,Dickson Claire L.2ORCID,Wei Ran2ORCID,Uhrín Dusan2ORCID,Butts Craig P.1ORCID

Affiliation:

1. School of Chemistry, University of Bristol, Cantocks Close, Bristol, BS8 1TS, UK

2. EaStCHEM School of Chemistry, University of Edinburgh, David Brewster Rd, Edinburgh EH9 3FJ, UK

Abstract

We extend the SHARPER NMR method designed to accommodate challenging reaction conditions to monitor simultaneously multiple resonances such as those of a reactant (2,6-difluoro-4-methoxyphenylboronic acid) and product (3,5-difluoroanisole).

Funder

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Electrochemistry,Spectroscopy,Environmental Chemistry,Biochemistry,Analytical Chemistry

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