Photoinduced reductive Reformatsky reaction of α-haloesters and aldehydes or ketones by cooperative dual-metal catalysis-Reference-Cited by-同舟云学术

Photoinduced reductive Reformatsky reaction of α-haloesters and aldehydes or ketones by cooperative dual-metal catalysis

Published:2023 Issue:97 Volume:59 Page:14427-14430
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Chen Qi-Long¹,Mao Le¹,Pan Yi-Fan¹,Cai Heng¹,Zhang Xiao-Ming¹^ORCID,Zhang Fu-Min¹^ORCID,Ma Ai-Jun²^ORCID,Peng Jin-Bao²^ORCID,Tu Yong-Qiang¹^ORCID

Affiliation:

1. State Key Laboratory of Applied Organic Chemistry & College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 730000, P. R. China

2. School of Biotechnology and Health Sciences, Wuyi University, Jiangmen, Guangdong 529020, P. R. China

Abstract

Combination of iron- and photocatalysis enables the development of a reductive Reformatsky reaction, providing a catalytic synthetic method to β-hydroxy esters from α-haloesters and aldehydes or ketones.

Funder

Fundamental Research Funds for the Central Universities

Beijing National Laboratory for Molecular Sciences

National Natural Science Foundation of China

Ministry of Education of the People's Republic of China

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2023/CC/D3CC04671K

Reference58 articles.

1. First Total Synthesis of a Natural Product Containing a Chiral, β-Diketone: Synthesis and Stereochemical Reassignment of Siphonarienedione and Siphonarienolone

2. Stereocontrolled Total Synthesis of (+)-Altohyrtin A/Spongistatin 1 Financial support was provided by the EPSRC (GR/L41646), Cambridge Commonwealth Trust (Scholarship to M.J.C.), EC (Marie Curie Postdoctoral Fellowship to J.L.A.), DFG (Postdoctoral Fellowship to T.T.), NSERC-Canada (Postdoctoral Fellowship to R.M.O.), Churchill College (Research Fellowship to D.J.W.), Kingapos;s College and Sims Fund, Cambridge (Scholarship to D.Y.K.C.). We also thank Merck and AstraZeneca Pharmaceuticals for generous support, and Dr. Anne Butlin (AZ) and Dr. Nick Bampos (Cambridge) for valuable assistance.

3. Exploring the Ring-Closing Metathesis for the Construction of the Solomonamide Macrocyclic Core: Identification of Bioactive Precursors

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5. Asymmetric total synthesis of pleurospiroketals A and B

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