Experimental study on the microreactor-assisted synthesis of phosphinic chlorides with varying steric hindrance-Reference-Cited by-同舟云学术

Experimental study on the microreactor-assisted synthesis of phosphinic chlorides with varying steric hindrance

Published:2020 Issue:22 Volume:7 Page:3664-3674
ISSN:2052-4129
Container-title:Organic Chemistry Frontiers
language:en
Short-container-title:Org. Chem. Front.

Author:

Jasiak Aleksandra¹²³⁴⁵^ORCID,Owsianik Krzysztof¹²³⁴⁵,Gostyński Bartłomiej¹²³⁴⁵^ORCID,Mielniczak Grażyna¹²³⁴⁵,Stevens Christian V.⁶⁷⁸⁹¹⁰^ORCID,Drabowicz Józef¹²³⁴⁵^ORCID

Affiliation:

1. Department of Organic Chemistry

2. Centre of Molecular and Macromolecular Studies

3. Polish Academy of Sciences

4. 90-363 Łódź

5. Poland

6. Department of Green Chemistry and Technology

7. Faculty of Bioscience Engineering

8. Ghent University

9. 9000 Gent

10. Belgium

Abstract

An efficient and catalyst-free method for the preparation of optically active and racemic mono-substituted t-butyl phosphinic chlorides ^tBuRP(O)Cl under flow conditions was reported.

Funder

Narodowe Centrum Nauki

Publisher

Royal Society of Chemistry (RSC)

Subject

Organic Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2020/QO/D0QO01129K

Reference50 articles.

1. Preparation of Scalemic P-Chiral Phosphines and Their Derivatives

2. Reduction of secondary and tertiary phosphine oxides to phosphines

3. An Overview of the Synthesis of Phosphinates and Phosphinic Amides

4. Stereospecific Halogenation of P(O)-H Bonds with Copper(II) Chloride Affording Optically Active Z1Z2P(O)Cl

5. Cobalt-Catalyzed Diastereoselective [4+2] Annulation of Phosphinamides with Heterobicyclic Alkenes at Room Temperature

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