Mechanochemical deprotection of <i>t</i>-butoxycarbonyl (Boc) group using basic alumina-Reference-Cited by-同舟云学术

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Mechanochemical deprotection of t-butoxycarbonyl (Boc) group using basic alumina

Published:2024 Issue: Volume: Page:
ISSN:1477-0520
Container-title:Organic & Biomolecular Chemistry
language:en
Short-container-title:Org. Biomol. Chem.

Author:

Tian Kaidi¹,Cai Tingna¹,Zhu Zedong¹,Cheng Kai¹^ORCID,Yu Lemao²^ORCID,Li Yong¹³^ORCID

Affiliation:

1. Zhejiang Key Laboratory of Alternative Technologies for Fine Chemicals Process, Shaoxing University, Shaoxing, 312000, China

2. Green Pharmaceuticals and Processes Research Centre, Shaoxing University, Shaoxing, 312000, China

3. State Key Laboratory of Medicinal Chemical Biology, College of Pharmacy, Nankai University, Tianjin, 300350, China

Abstract

A solvent-free, operationally simple, and chemoselective mechanochemical method for t-butoxycarbonyl (Boc) deprotection is described.

Funder

National Natural Science Foundation of China

State Key Laboratory of Medicinal Chemical Biology

Nankai University

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/OB/D4OB01091D

Reference59 articles.

1. Oxidative Reactions of Hydrazines. II. Isophthalimides. New Protective Groups on Nitrogen1,2

2. Synthetic Approaches to the New Drugs Approved During 2020

3. Synthetic Approaches to the New Drugs Approved During 2021

4. Tertiary-butoxycarbonyl (Boc) – A strategic group for N-protection/deprotection in the synthesis of various natural/unnatural N-unprotected aminoacid cyanomethyl esters

5. Total synthesis of galantin I. Acid-catalyzed cyclization of galantinic acid

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