“Perfecting” pure shift HSQC: full homodecoupling for accurate and precise determination of heteronuclear couplings-Reference-Cited by-同舟云学术

“Perfecting” pure shift HSQC: full homodecoupling for accurate and precise determination of heteronuclear couplings

Published:2014 Issue:99 Volume:50 Page:15702-15705
ISSN:1359-7345
Container-title:Chem. Commun.
language:en
Short-container-title:Chem. Commun.

Author:

Kaltschnee L.¹²³,Kolmer A.¹²³,Timári I.⁴⁵⁶,Schmidts V.¹²³,Adams R. W.⁷⁸⁹^ORCID,Nilsson M.⁷⁸⁹¹⁰¹¹,Kövér K. E.⁴⁵⁶,Morris G. A.⁷⁸⁹,Thiele C. M.¹²³

Affiliation:

1. Clemens-Schöpf-Institut für Organische Chemie und Biochemie

2. Technische Universität Darmstadt

3. D-64287 Darmstadt, Germany

4. Department of Inorganic and Analytical Chemistry

5. University of Debrecen

6. H-4032 Debrecen, Hungary

7. School of Chemistry

8. University of Manchester

9. Manchester M13 9PL, UK

10. Department of Food Science

11. University of Copenhagen

Abstract

Full suppression of proton–proton couplings in pure shift HSQC spectra simplifies their analysis, as demonstrated for high precision RDC measurements.

Funder

European Research Council

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2014/CC/C4CC04217D

Reference34 articles.

1. Pure shift proton DOSY: diffusion-ordered 1H spectra without multiplet structure

2. Experimental access to HSQC spectra decoupled in all frequency dimensions

3. Simplifying Proton NMR Spectra by Instant Homonuclear Broadband Decoupling

4. Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy

5. Toward single-shot pure-shift solution 1H NMR by trains of BIRD-based homonuclear decoupling

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