A novel electrochemical flow-cell for operando XAS investigations in X-ray opaque supports

Author:

Paparoni Francesco12ORCID,Alizon Guillaume1,Zitolo Andrea1ORCID,Rezvani Seyed Javad23,Di Cicco Andrea2ORCID,Magnan Hélène4ORCID,Fonda Emiliano1ORCID

Affiliation:

1. Synchrotron SOLEIL, Départementale 128, 91190 Saint-Aubin, France

2. Sez. Fisica, Scuola di Scienze e Tecnologie, Universitá di Camerino, via Madonna delle Carceri, I-62032 Camerino, Italy

3. CNR-IOM, SS14 – km 163.5 in Area Science Park, 34149, Trieste, Italy

4. Université Paris-Saclay, CEA, CNRS, Service de Physique de l’Etat Condensé, F-91191 Gif-sur-Yvette, France

Abstract

Electrochemical cell for operando XAS measurements down to the Ti K edge. Sample is probed from the electrolyte side. As a case study, we investigated Ni-doped maghemite epitaxially grown on Pt as a catalyst for the oxygen evolution reaction.

Funder

Agence Nationale de la Recherche

Publisher

Royal Society of Chemistry (RSC)

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