Dynamic nuclear polarisation enhanced14N overtone MAS NMR spectroscopy
Author:
Affiliation:
1. Centre de RMN à Trés Hauts Champs
2. Institut de Sciences Analytiques
3. Université de Lyon (CNRS/ENS Lyon/UCB Lyon 1)
4. 69100 Villeurbanne, France
5. Institute for Frontier Materials
6. Deakin University
7. Geelong, Australia
Abstract
Dynamic nuclear polarisation has been used to obtain solid-state14N overtone NMR spectra with signal enhancement levels of over two orders of magnitude, including natural abundance C–N and H–N correlation spectra.
Publisher
Royal Society of Chemistry (RSC)
Subject
Physical and Theoretical Chemistry,General Physics and Astronomy
Link
http://pubs.rsc.org/en/content/articlepdf/2014/CP/C4CP00590B
Reference48 articles.
1. Direct detection of nitrogen-14 in solid-state NMR spectroscopy
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5. Measuring Amide Nitrogen Quadrupolar Coupling by High-Resolution 14N/13C NMR Correlation under Magic-Angle Spinning
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