Ag-Catalyzed difluorohydration of β-alkynyl ketones for diastereoselective synthesis of 1,5-dicarbonyl compounds-Reference-Cited by-同舟云学术

Ag-Catalyzed difluorohydration of β-alkynyl ketones for diastereoselective synthesis of 1,5-dicarbonyl compounds

Published:2017 Issue:48 Volume:53 Page:6397-6400
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Zhu Yi-Long¹²³⁴⁵,Wang Ai-Fang¹²³⁴⁵,Du Jian-Yu¹²³⁴⁵,Leng Bo-Rong⁶⁷⁸⁵,Tu Shu-Jiang¹²³⁴⁵,Wang De-Cai⁶⁷⁸⁵,Wei Ping⁶⁷⁸⁵,Hao Wen-Juan¹²³⁴⁵,Jiang Bo¹²³⁴⁵^ORCID

Affiliation:

1. School of Chemistry and Materials Science

2. Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials

3. Jiangsu Normal University

4. Xuzhou 221116

5. P. R. China

6. Biotechnology and Pharmaceutical Engineering

7. Nanjing Tech University

8. Nanjing 210009

Abstract

A new catalytic difluorohydration of β-alkynyl ketones using NFSI as the fluorinating reagent has been established, diastereoselectively providing difluoride 1,5-dicarbonyl products, and some of them were converted into difluorinated isoquinolines.

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2017/CC/C7CC02088K

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