In situ electron tomography for the thermally activated solid reaction of anaerobic nanoparticles

Author:

Ihara Shiro1ORCID,Yoshinaga Mizumo2,Miyazaki Hiroya3,Wada Kota2,Hata Satoshi24ORCID,Saito Hikaru15ORCID,Murayama Mitsuhiro167ORCID

Affiliation:

1. Institute for Materials Chemistry and Engineering, Kyushu University, Fukuoka 816-8580, Japan

2. Interdisciplinary Graduate School of Engineering Sciences, Kyushu University, Fukuoka 816-8580, Japan

3. Mel-Build Corporation, Nishi-ku, Fukuoka 819-0052, Japan

4. The Ultramicroscopy Research Center, Kyushu University, Fukuoka 819-0395, Japan

5. Pan-Omics Data-Driven Research Innovation Center, Kyushu University, Fukuoka 816-8580, Japan

6. Department of Materials Science and Engineering, Virginia Tech, Blacksburg, VA 24061, USA

7. Reactor Materials and Mechanical Design Group, Energy and Environmental Directorate, Pacific Northwest National Laboratory, WA 99352, USA

Abstract

A newly developed in situ electron tomography visualizes an entire process of Cu nanoparticle sintering in 4D (3D real space and time) from its very initial stage to the densification of nanoparticle clusters.

Funder

Japan Society for the Promotion of Science

Iketani Science and Technology Foundation

Core Research for Evolutional Science and Technology

Institute for Critical Technology and Applied Science

Virginia Polytechnic Institute and State University

National Science Foundation

Publisher

Royal Society of Chemistry (RSC)

Subject

General Materials Science

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