Design and synthesis of versatile ligand precursors based on phosphonium ylides for palladalactam formation and catalytic investigation-Reference-Cited by-同舟云学术

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Design and synthesis of versatile ligand precursors based on phosphonium ylides for palladalactam formation and catalytic investigation

Published:2024 Issue:25 Volume:53 Page:10475-10485
ISSN:1477-9226
Container-title:Dalton Transactions
language:en
Short-container-title:Dalton Trans.

Author:

Kao Cheng-Po¹,Lee Jhen-Yi¹,Tang Min-Cheng¹,Lee Hon Man¹^ORCID

Affiliation:

1. Department of Chemistry, National Changhua University of Education, Changhua, 500, Taiwan

Abstract

A novel series of ligand precursors for palladalactams has been developed. A synthesized palladalactam with an electron-donating PEt3 moiety shows promising catalytic activity in Mizoroki–Heck coupling, supported by theoretical calculations.

Funder

National Science and Technology Council

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/DT/D4DT00862F

Reference58 articles.

1. Phosphorus Ylides in the Coordination Sphere of Transition Metals: An Inventory

2. Synthesis of mono- and di-nuclear palladium(II) complexes containing ylide ligands [PPh2(CHCO2R)2]–(R = Me or Et). Crystal structures of [Pd{(CHCO2Et)2PPh2}2], [Pd{(CHCO2Et)2PPh2}Cl(PPh3)], and [Pd{(CHCO2Et)2PPh2}(NC5H5)2]ClO4

3. Synthesis and Structure of PdII Complexes Containing the C,C-Chelating Bis-Ylide Ligand [Ph3PC(H)]2CO. X-ray Crystal Structure of {Pd(μ-Cl){[C(H)PPh3]2CO}}2(ClO4)2·CH2Cl2

4. Ligand-Induced and Thermally-Induced Orthometalation of the Bis(ylide) Ligand [Ph3PC(H)]2CO. Generation of the C,C-Chelating Group C6H4-2-PPh2C((H)COCH2PPh3

5. Palladium(II) Complexes of α-Stabilized Phosphorus Ylides

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