High-resolution polymer high performance liquid chromatography: optimization of the saw tooth gradient profile for various stationary phases and separations on preparative scale-Reference-Cited by-同舟云学术

High-resolution polymer high performance liquid chromatography: optimization of the saw tooth gradient profile for various stationary phases and separations on preparative scale

Published:2019 Issue:39 Volume:11 Page:4960-4968
ISSN:1759-9660
Container-title:Analytical Methods
language:en
Short-container-title:Anal. Methods

Author:

Durner Bernhard¹²³⁴⁵^ORCID,Ehmann Thomas¹²³,Matysik Frank-Michael⁴⁵⁶³

Affiliation:

1. Wacker Chemie AG

2. Burghausen

3. Germany

4. Department of Chemistry and Pharmacy

5. University of Regensburg

6. 93040 Regensburg

Abstract

The recently introduced saw tooth gradient protocol for high-resolution polymer HPLC was further improved and optimized in terms of total runtime and separation performance.

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2019/AY/C9AY00689C

Reference23 articles.

1. Y. Brun and C. J.Rasmussen , Interaction polymer chromatography , in Liquid chromatography: Fundamentals and instrumentation , ed. S. Fanali , P. R. Haddad , C.F. Poole and M.-L. Riekkola , 2 nd edn, Elsevier , Amsterdam, Netherlands, Oxford, United Kingdom, Cambridge, MA, United States , 2017 , pp. 275–318

2. H. Pasch and B.Trathnigg , Multidimensional HPLC of polymers , Springer Laboratory: Manuals in Polymer Science , Springer, Berlin, Heidelberg , 2013

3. H. Pasch and B.Trathnigg , HPLC of polymers , Springer Laboratory , Springer, Berlin , 1998

4. D. Berek , Polymer HPLC , in Handbook of HPLC , ed. D. Corradini , 2 nd edn, CRC Press , Boca Raton, FL , 2010 , pp. 447–504

5. G. Glöckner , Gradient HPLC of copolymers and chromatographic cross-fractionation , Springer , Berlin, Heidelberg , 1991