Solid-state <sup>17</sup>O NMR study of α-<scp>d</scp>-glucose: exploring new frontiers in isotopic labeling, sensitivity enhancement, and NMR crystallography-Reference-Cited by-同舟云学术

Solid-state ¹⁷O NMR study of α-d-glucose: exploring new frontiers in isotopic labeling, sensitivity enhancement, and NMR crystallography

Published:2022 Issue:9 Volume:13 Page:2591-2603
ISSN:2041-6520
Container-title:Chemical Science
language:en
Short-container-title:Chem. Sci.

Author:

Shen Jiahui¹,Terskikh Victor²^ORCID,Struppe Jochem³^ORCID,Hassan Alia⁴,Monette Martine⁵,Hung Ivan⁶^ORCID,Gan Zhehong⁶^ORCID,Brinkmann Andreas²^ORCID,Wu Gang¹^ORCID

Affiliation:

1. Department of Chemistry, Queen's University, 90 Bader Lane, Kingston, Ontario K7L 3N6, Canada

2. Metrology, National Research Council Canada, Ottawa, Ontario K1A 0R6, Canada

3. Bruker Biospin Corporation, 15 Fortune Drive, Billerica, MA 01821, USA

4. Bruker Switzerland AG, Fällanden, Switzerland

5. Bruker Biospin Ltd., 2800 High Point Drive, Suite 206, Milton, Ontario L9T 6P4, Canada

6. National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, Florida 32310, USA

Abstract

We report the first “total synthesis” of 17O-labeled d-glucose and its solid-state 17O NMR characterization with unprecedented sensitivity and resolution.

Funder

Natural Sciences and Engineering Research Council of Canada

National Science Foundation

Publisher

Royal Society of Chemistry (RSC)

Subject

General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2022/SC/D1SC06060K

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1. Recent developments in solid-state nuclear magnetic resonance of quadrupolar nuclei and applications to biological systems

2. A review of oxygen-17 solid-state NMR of organic materials—towards biological applications