Synthesis of poly(methylsilsesquioxane-<i>co</i>-dimethylsiloxane) liquids and deep-ultraviolet transparent elastic resins through co-solvent-free water-rich hydrolytic polycondensation of organoalkoxysilanes-Reference-Cited by-同舟云学术

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Synthesis of poly(methylsilsesquioxane-co-dimethylsiloxane) liquids and deep-ultraviolet transparent elastic resins through co-solvent-free water-rich hydrolytic polycondensation of organoalkoxysilanes

Published:2024 Issue:19 Volume:15 Page:1937-1941
ISSN:1759-9954
Container-title:Polymer Chemistry
language:en
Short-container-title:Polym. Chem.

Author:

Yoshida Takuma¹,Ishijima Masanao¹^ORCID,Yoshida Satoshi²^ORCID,Koike Akio²,Kajihara Koichi¹^ORCID

Affiliation:

1. Department of Applied Chemistry for Environment, Graduate School of Urban Environmental Sciences, Tokyo Metropolitan University, 1-1 Minami-Osawa, Hachioji, Tokyo 192-0397, Japan

2. Materials Integration Laboratories, AGC Inc., 1-1 Suehiro-cho, Tsurumi-ku, Yokohama, Kanagawa 230-0045, Japan

Abstract

A co-solvent-free hydrolytic polycondensation of mono- and dimethylmethoxysilanes at high H2O/Si ratios (≳10) gave methylsilsesquioxane-rich (80 mol%) liquids heat-curable to stiff, tough, and deep-UV transparent resins showing full elastic recovery.

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/PY/D4PY00146J

Reference31 articles.

1. New type of non-crystalline solids between inorganic and organic materials

2. Silsesquioxanes

3. Organic/Inorganic Hybrid Network Materials by the Sol−Gel Approach

4. Oligo- and polysiloxanes

5. Applications of hybrid organic–inorganic nanocomposites

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