Challenges for the determination of spiramycin in aqueous matrices using LC-MS/MS: evidence for the solvent intrusion on the molecule integrity-Reference-Cited by-同舟云学术

Challenges for the determination of spiramycin in aqueous matrices using LC-MS/MS: evidence for the solvent intrusion on the molecule integrity

Published:2022 Issue:27 Volume:12 Page:17096-17103
ISSN:2046-2069
Container-title:RSC Advances
language:en
Short-container-title:RSC Adv.

Author:

Nasiri Azadeh¹²^ORCID,Mokhtari Shaya³⁴^ORCID,Jahani Reza¹^ORCID,Daraie Bahram¹,Yazdanpanah Hassan¹²,Faizi Mehrdad¹,Kobarfard Farzad³⁴⁵

Affiliation:

1. Department of Pharmacology and Toxicology, School of Pharmacy, Shahid Beheshti University of Medical Sciences, Tehran, Iran

2. Food Safety Research Center, Shahid Beheshti University of Medical Sciences, Tehran, Iran

3. Central Research Laboratories, Shahid Beheshti University of Medical Sciences, Tehran, Iran

4. Phytochemistry Research Center, Shahid Beheshti University of Medical Sciences, Tehran, Iran

5. Department of Medicinal Chemistry, School of Pharmacy, Shahid Beheshti University of Medical Sciences, Tehran, Iran

Abstract

Water, ethanol, and methanol as protic solvents can add to the formyl group of spiramycin molecules during standard solutions preparation while there was no evidence for the addition of acetonitrile and dimethyl sulfoxide as aprotic solvents.

Publisher

Royal Society of Chemistry (RSC)

Subject

General Chemical Engineering,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2022/RA/D2RA00205A

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5. Synthesis and Use of Stable-Isotope-Labeled Internal Standards for Quantification of Phosphorylated Metabolites by LC–MS/MS

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