Development of a simple and rapid EDXRF method for quantification of ZrO2 and HfO2 in aqueous and organic process stream solutions generated from a zirconium extraction facility

Author:

Balaji Rao Y.1ORCID,NVMS Gupta S.1,V. Nagendra Kumar P.2,Srivastava Dinesh1

Affiliation:

1. Nuclear Fuel Complex, Dept of Atomic Energy, ECIL post, Hyderabad 500062, India

2. Dept of Chemistry, GITAM University, Hyderabad 502329, India

Abstract

The present work highlights the customization of an EDXRF analyzer with a specially designed sample cell/holder to facilitate analysis of aqueous/organic process sample solutions with wide concentration range from a zirconium extraction facility.

Publisher

Royal Society of Chemistry (RSC)

Reference20 articles.

1. C.Ganguly , Advances in Zircoinium Technology for Nuclear Reactor Application , Presented in ZIRC-2002, BARC , Mumbai, India , September, 2002

2. TSanyal , Zirconium technology for cladding and calandria tubes , IANCAS bulletin , 2005 , IV ( 3 ), 191204

3. A. K.Mukherji , Chapter-4: Gravimetric Determinations , Analytical Chemistry of Zirconium and Hafnium , 1970 , vol. 40 , pp. 18–44

4. C. A.Majid , M. A.Hussain and K.Saeed , Quantitative Microanalysis of Hafnium – Zirconium System by X-Ray Fluorescene , PINSTECH/NMD-115

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