Real-time reaction monitoring by ultrafast 2D NMR on a benchtop spectrometer

Author:

Gouilleux Boris12345,Charrier Benoît12345,Danieli Ernesto6789,Dumez Jean-Nicolas1011125,Akoka Serge12345,Felpin François-Xavier12345,Rodriguez-Zubiri Mireia12345,Giraudeau Patrick12345

Affiliation:

1. CEISAM CNRS

2. UMR6230

3. Université de Nantes

4. 44322 Nantes

5. France

6. Institut für Technische und Makromolekulare Chemie (ITMC)

7. RWTH Aachen University

8. 52074 Aachen

9. Germany

10. CNRS UPR2301

11. Institut de Chimie des Substances Naturelles

12. 91198 Gif-sur-Yvette Cedex

Abstract

Ultrafast 2D NMR spectra are recorded on a compact spectrometer to follow in real time a reaction in the synthetic chemistry laboratory. Complex reactions can be monitored in non-deuterated solvents to confirm in real time the molecular structure of the compounds involved in the reaction while giving access to relevant kinetic parameters.

Publisher

Royal Society of Chemistry (RSC)

Subject

Electrochemistry,Spectroscopy,Environmental Chemistry,Biochemistry,Analytical Chemistry

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