Mixed lead carboxylates relevant to soap formation in oil and tempera paintings: the study of the crystal structure by complementary XRPD and ssNMR

Author:

Kočí Eva1234,Rohlíček Jan564,Kobera Libor784ORCID,Plocek Jiří1234,Švarcová Silvie1234ORCID,Bezdička Petr1234ORCID

Affiliation:

1. Institute of Inorganic Chemistry of the Czech Academy of Sciences

2. ALMA Laboratory

3. 250 68 Husinec-Řež

4. Czech Republic

5. Institute of Physics of the Czech Academy of Sciences

6. 182 21 Prague 8

7. Institute of Macromolecular Chemistry of the Czech Academy of Sciences

8. 162 06 Praha 6

Abstract

The crystal structure of mixed lead carboxylates consisting of both palmitate and stearate anions was revealed by complementary XRPD and ssNMR.

Funder

Grantová Agentura České Republiky

Publisher

Royal Society of Chemistry (RSC)

Subject

Inorganic Chemistry

Reference40 articles.

1. N. Eastaugh , V.Walsh , T.Chaplin and R.Siddall , The Pigment Compendium, A Dictionar of Historical Pigments , Elsevier , 2004

2. Degradation of lead-based pigments by salt solutions

3. A study on red lead degradation in a medieval manuscript Lorvão Apocalypse (1189)

4. Analytical Imaging Studies of Cross-Sections of Paintings Affected by Lead Soap Aggregate Formation

5. A. Van Loon , P.Noble and A.Burnstock , in Conservation of Easel Paintings , ed. J. Hill Stoner and R. Rushfield , London and New York , 2012 , pp. 214–241

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