Combination of near-infrared spectroscopy and a transient flow method for efficient kinetic analysis of the Claisen rearrangement

Author:

Takebayashi Yoshihiro1ORCID,Sue Kiwamu1,Kataoka Sho1ORCID

Affiliation:

1. Research Institute for Chemical Process Technology, National Institute of Advanced Industrial Science and Technology (AIST), 1-1-1 Higashi, Tsukuba, Ibaraki 305-8565, Japan

Abstract

An automated flow reactor with a rapid inline monitoring using a compact near-infrared spectrometer and a flow rate ramp control enabled high-density kinetic data acquisition.

Funder

New Energy and Industrial Technology Development Organization

Publisher

Royal Society of Chemistry (RSC)

Reference54 articles.

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3. Flow Chemistry: Integrated Approaches for Practical Applications , ed. S. V. Luis and E. Garcia-Verdugo , Royal Society of Chemistry , 2019

4. Flow Chemistry: Fundamentals and Applications , ed. F. Darvas , G. Dorman , V. Hessel and S. V. Ley , De Gruyter , 2nd edn, 2021

5. Flow and Microreactor Technology in Medicinal Chemistry , ed. E. Alza , Wiley-VCH , 2022

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