A Johann-type X-ray emission spectrometer at the Rossendorf beamline

Abstract

This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5–25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°–89°. The instrument has been tested at high and intermediate incident energies,i.e.at the ZrK-edge and at the AuL3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.