Mechanical stretching of a perfect single crystal: a routeway to a d-spacing tunable X-ray monochromator

Author:

Cusatis CesarORCID,Piragibe Barros Silva Borges Egon,Tirao Germán Alfredo,Honnicke Marcelo GoncalvesORCID

Abstract

The feasibility of using traction forces to produce mechanical stretching/shrinkage in a perfect Si 400 single crystal is explored theoretically (by finite element analysis and dynamical theory of X-ray diffraction) and experimentally in order to use it as an angular static interplanar-distance (d-spacing) tunable monochromator, in the Bragg case. It is shown that, with traction forces of ∼100 N and an appropriate pre-load, it is possible to scan, with a linear response and reproducibility of ∼5%, a 30 eV bandwidth, which corresponds to a d-spacing scan of 7 × 10−3 Å.

Funder

Conselho Nacional de Desenvolvimento Científico e Tecnológico

PSAP/ILACVN/UNILA

Publisher

International Union of Crystallography (IUCr)

Subject

General Biochemistry, Genetics and Molecular Biology

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