Multi-tube area detector developed for reactor small-angle neutron scattering spectrometer SANS-J-II

Abstract

A newly developed multi-tube area detector for a small-angle neutron scattering (SANS) spectrometer (SANS-J-II) at the research reactor JRR-3 in Tokai, Japan, has been implementedviathe use of one-dimensional position-sensitive3He detectors (tubes). Ninety-six active tubes of 8 mm in diameter and 650 and 580 mm in length were filled with 15 atm (1.52 MPa) of3He and aligned vertically parallel in order to cover a sufficiently large area for small-angle scattering measurement. These tubes are enclosed in an air chamber together with neutron encode and GATENET modules (VME boards), which compose a standard data acquisition system for the spallation neutron source of the Japan Proton Accelerator Research Complex. This system facilitates the acquisition of time-of-flight neutron event data. The multi-tube detector is mounted on a truck moving in a vacuum chamber of the SANS spectrometer. After discriminating noise originating from γ-rays, and calibrating the positions and sensitivities of individual tubes, the resolution was determined (i.e.channel widths along parallel and vertical directions along a tube). The counting rate of one tube was determined to be 1.4 × 103counts per second with a counting loss of 1%. This implies that the new detector, composed of 96 tubes, can detect more than 105neutrons per second with a counting loss of 1%. To demonstrate its use, small-angle scattering originating from a diblock copolymer film with a highly oriented lamellar microdomain was observed. The data acquisition in event mode has a great advantage in time-resolved measurements that are synchronized with external stimuli imposed on a sample.