IndiumKα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation

Author:

Graw NicoORCID,Ruth Paul NiklasORCID,Ernemann Tobias,Herbst-Irmer RegineORCID,Stalke DietmarORCID

Abstract

The MetalJet X-ray source provides indiumKα radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrated that these data can be used in the refinement of a multipole model, the results of which are used for a topological analysis to assess the bonding situation in a sulfur ylide compound.

Funder

Deutsche Forschungsgemeinschaft

Publisher

International Union of Crystallography (IUCr)

Subject

General Biochemistry, Genetics and Molecular Biology

Cited by 2 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. In data we trust: X-ray diffraction experiments for charge density investigations;Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials;2023-09-19

2. Indium Kα radiation from a MetalJet X-ray source: comparison of the Eiger2 CdTe and Photon III detectors;Journal of Applied Crystallography;2023-09-05

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