Author:
Takahashi Yasuhiko,Ohshima Ken-ichi,Yamamoto Kazuki,Yukino Ken,Okamura Fujio P.
Abstract
An accurate structure analysis of a spherical LaB6single crystal has been performed with the use of short-wavelength X-rays (WKα1) in order to estimate the termination effect in Fourier synthesis on the electron-density distribution (EDD). It is concluded that the effect on the EDD is negligible if data are taken up to \sin \theta /\lambda =2.0 Å−1, because the negative values disappear completely from the map. The values of displacement parameters of the constituent atoms in LaB6are also discussed.
Publisher
International Union of Crystallography (IUCr)
Subject
General Biochemistry, Genetics and Molecular Biology
Cited by
2 articles.
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