Author:
Okmanov R. Ya.,Tukhtaev D. B.,Saidov A. Sh.,Tashkhodjaev B.
Abstract
The molecular salt, C23H26N2O2
+·Cl−, was obtained from 1-isobutyl-8,9-dimethoxy-3-phenyl-5,6-dihydroimidazo[5,1-a]isoquinoline, which was synthesized by cyclocondensation of α-benzoylamino-γ-methyl-N-[2-(3,4-dimethoxyphenyl)ethyl]valeramide in the presence of phosphoryl chloride. The tetrahydropyridine ring adopts a twist–boat conformation. In the crystal structure, centrosymmetric dimers are formed by N—H...Cl and C—H...Cl hydrogen bonds.
Funder
Academy of Sciences of the Republic of Uzbekistan
Publisher
International Union of Crystallography (IUCr)
Subject
Rehabilitation,Physical Therapy, Sports Therapy and Rehabilitation,General Medicine
Reference10 articles.
1. Synthetic applications of aryl radical building blocks for cyclisation onto azoles
2. Bruker (1998). XP. Bruker AXS Inc., Madison, Wisconsin, USA.
3. Bruker (2008). SADABS. Bruker AXS Inc., Madison, Wisconsin, USA.
4. Transition-Metal-Catalyzed Arylation of Nitroimidazoles and Further Transformations of Manipulable Nitro Group
5. Rigaku OD (2018). CrysAlis PRO. Rigaku OD, Yarnton, England.