[1–9-NαC]-Linusorb B3 (Cyclolinopeptide A) dimethyl sulfoxide monosolvate

Author:

Purdy Sarah KendraORCID,Spasyuk Denis,Chitanda Jackson Mulenga,Reaney Martin J. T.

Abstract

Crystals of the dimethyl sulfoxide (DMSO) solvate of [1–9-NαC]-linusorb B3 (Cyclolinopeptide A; CLP-A; C57H84N9O9·C2H6OS), a cyclic polypeptide were obtained following peptide extraction and purification from flaxseed oil. There are four intramolecular N—H...O hydrogen bonds. In the crystal, the molecules are linked in chains along the a axis by N—H...O hydrogen bonds. Each DMSO O atom accepts a hydrogen bond from an NH group at the Phe6 location in the CLP-A molecule.

Funder

Saskatchewan Agricultural Development Fund

Natural Sciences and Engineering Research Council of Canada

Canada Foundation for Innovation

National Research Council of Canada

Canadian Institute for Health Research

Government of Saskatchewan

University of Saskatchewan

Publisher

International Union of Crystallography (IUCr)

Subject

Rehabilitation,Physical Therapy, Sports Therapy and Rehabilitation,General Medicine

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