Focal construct geometry – a novel approach to the acquisition of diffraction data

Author:

Rogers Keith,Evans Paul,Rogers Joseph,Chan JerWang,Dicken Anthony

Abstract

This paper presents the first use of a simple novel geometry that enables the measurement of diffractograms from polycrystalline materials through linear translation of a point detector. The geometry is such that intensities from all points around any Debye ring are summed to a single point, and thus coherently scattered X-rays are harvested efficiently. Data from initial experimental verification of the approach used in transmission mode are presented and the diffractograms compared with their equivalent measured using a pencil beam. Brief discussions of potential modifications in reflection geometry and applications for fibre samples are also provided.

Publisher

International Union of Crystallography (IUCr)

Subject

General Biochemistry, Genetics and Molecular Biology

Reference8 articles.

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