(Z)-3-[2-(2,4-Dinitrophenyl)hydrazin-1-ylidene]isobenzofuran-1(3H)-one dichloromethane hemisolvate-Reference-Cited by-同舟云学术

(Z)-3-[2-(2,4-Dinitrophenyl)hydrazin-1-ylidene]isobenzofuran-1(3H)-one dichloromethane hemisolvate

Published:2014-03-12 Issue:4 Volume:70 Page:o418-o418
ISSN:1600-5368
Container-title:Acta Crystallographica Section E Structure Reports Online
language:
Short-container-title:Acta Cryst E

Author:

Agarwal Palak,Mishra Pragati,Gupta Nikita,Neelam ,Sahoo Priyaranjan,Kumar Satish

Abstract

In the title compound, 2C14H8N4O6·CH2Cl2, the dichloromethane solvent molecule resides on a crystallographic twofold axis. The mean plane of the phthalisoimide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intramolecular N—H...O hydrogen bond occurs. The crystal packing features a short Cl...O halogen-bond interaction [3.093 (3) Å].

Publisher

International Union of Crystallography (IUCr)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

http://journals.iucr.org/e/issues/2014/04/00/fj2664/fj2664.pdf

Reference12 articles.

1. Agilent (2011). CrysAlis PRO. Agilent Technologies Ltd, Yarnton, England.

2. Reactions of amines or amides with phthaloyl chloride. Synthesis of flourine-containing N,N-dimethyl-N′-substituted amidines and related compounds

3. OLEX2: a complete structure solution, refinement and analysis program

4. Crystal-to-crystal transformation amongst dimorphs of racemic 2,6-di-O-(p-halo benzoyl)-myo-inositol 1,3,5-orthoformates that achieves halogen bonding contacts

5. The reaction of phthalidylidene dichloride with primary amines. Synthesis and X-ray molecular structure of N-substituted phthalisoimides

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