Crystallographic characterization of (C5H4SiMe3)3U(BH4)

Author:

Windorff Cory J.,Cross Justin N.ORCID,Scott Brian L.ORCID,Kozimor Stosh A.ORCID,Evans William J.

Abstract

New syntheses have been developed for the synthesis of (borohydrido-κ3 H)tris[η5-(trimethylsilyl)cyclopentadienyl]uranium(IV), [U(BH4)(C8H13Si)3] or Cp′3U(BH4) (Cp′ = C5H4SiMe3) and its structure has been determined by single-crystal X-ray crystallography. This compound crystallized in the space group P\overline{1} and the structure features three η 5-coordinated Cp′ rings and a κ 3-coordinated (BH4) ligand.

Publisher

International Union of Crystallography (IUCr)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

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