Crystal structure and Hirshfeld surface analysis of a new mononuclear copper(II) complex: [bis(pyridin-2-yl-κN)amine](formato-κO)(m-hydroxybenzoato-κ2 O,O′)copper(II)

Author:

Chaisuriya Wanassanan,Chainok Kittipong,Wannarit NanthawatORCID

Abstract

A new mononuclear copper(II) complex, [Cu(C7H5O3)(HCO2)(C10H9N3)], containing mixed N- and O-donor ligands, 2,2′-dipyridylamine (dpyam) and m-hydroxybenzoate (m-OHbenz), has been obtained from a solvent mixture. The coordination environment of the CuII ion is distorted square-pyramidal with a [N2O3] coordination set originating from the chelating dpyam and m-OHbenz ligands in the basal plane and the O atom of a formato ligand at the apical position. The crystal structure of the title complex is stabilized by N—H...O, O—H...O, C—H...O hydrogen-bonding, π–π and C—H...π intermolecular interactions, which were quantified by Hirshfeld surface analysis.

Funder

Department of Chemistry, Faculty of Science and Technology, Thammasat University, Thailand

Thammasat University Research Unit in Multifunctional Crystalline Materials and Applications Research Unit

Publisher

International Union of Crystallography (IUCr)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

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