Crystal structure of 2,3-dimethoxy-5,6,7,8,13,13a-hexahydro-6a,8-diazaindeno[2,1-b]phenanthrene methanol monosolvate
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Published:2015-07-15
Issue:8
Volume:71
Page:o574-o575
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ISSN:2056-9890
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Container-title:Acta Crystallographica Section E Crystallographic Communications
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language:
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Short-container-title:Acta Cryst E
Author:
Adizov Shahobiddin M.,Saidov Abdusalom Sh.,Turgunov Kambarali K.,Okmanov Rasul Ya.,Tashkhodjaev Bakhodir
Abstract
The asymmetric unit of the title solvate, C21H22N2O2·CH3OH, contains one methanol solvent molecule and one molecule of the heterocycle that is built up by the fusion of four six-membered ringsA,C,D,Eand one five-membered ringB. The indole moiety (ringsAandB) is essentially planar, with an r.m.s. deviation of 0.013 Å, whereas ringsCandDadopt a twisted conformation with atrans-ring junction. In the crystal, two heterocyclic molecules are associated with two methanol molecules through mutual N—H...O and O—H...N hydrogen bonds, forming a centrosymmetric dimer.
Publisher
International Union of Crystallography (IUCr)
Subject
Condensed Matter Physics,General Materials Science,General Chemistry
Cited by
1 articles.
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