Lab-scale production of anhydrous diazomethane using membrane separation technology
Author:
Publisher
Springer Science and Business Media LLC
Subject
General Biochemistry, Genetics and Molecular Biology
Link
http://www.nature.com/articles/nprot.2017.046.pdf
Reference37 articles.
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3. Pace, V., Verniest, G., Sinisterra, J.-V., Alcántara, A.R. & De Kimpe, N. Improved Arndt-Eistert synthesis of α-diazoketones requiring minimal diazomethane in the presence of calcium oxide as acid scavenger. J. Org. Chem. 75, 5760–5763 (2010).
4. Candeias, N.R., Paterna, R. & Gois, P.M.P. Homologation reaction of ketones with diazo compounds. Chem. Rev. 116, 2937–2981 (2016).
5. Schjøth-Eskesen, C. & Jensen, H.H. Efficient Arndt–Eistert synthesis of selective 5-HT7 receptor antagonist SB-269970. Synth. Commun. 39, 3243–3253 (2009).
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