Continuous Production of the Diazomethane Precursor N-Methyl-N-nitroso-p-toluenesulfonamide: Batch Optimization and Transfer into a Microreactor Setup-Reference-Cited by-同舟云学术

Continuous Production of the Diazomethane Precursor N-Methyl-N-nitroso-p-toluenesulfonamide: Batch Optimization and Transfer into a Microreactor Setup

Published:2009-08-31 Issue:5 Volume:13 Page:1014-1021
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Struempel Michael¹,Ondruschka Bernd¹,Stark Annegret¹

Affiliation:

1. Friedrich-Schiller University Jena, Institute for Technical Chemistry and Environmental Chemistry, Lessingstrasse 12, 07743 Jena, Germany

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/op900081g

Reference29 articles.

1. Diazald in chemical synthesis:http://www.sigmaaldrich.com/chemistry/chemical-synthesis/technology-spotlights/diazald.html; accessed 10 January 2009.

2. Diazald, MNNG and Diazomethane Generators, Aldrich Technical Bulletin, AL-180.

3. Archibald, T. G.Large Scale Batch Process for Diazomethane. (Aerojet-General Corporation).U.S. Patent 5,817,778, 1997.

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