1. Centre Interuniversitaire de Recherche d'Ingénierie sur les Matériaux, Université Paul Sabatier, UMR CNRS 5085, Bât. 2Rl, 31062 Toulouse Cedex 9, France, Inorganic Chemistry Laboratory and Department of Materials, University of Oxford, Parks Road, Oxford, OX1 3PH, United Kingdom, and Department of Chemistry, University Science Laboratories, South Road, Durham, DH1 3LE, United Kingdom