Synthesis of 13C-Perlabeled Cellulose with more than 99% Isotopic Enrichment by a Cationic Ring-Opening Polymerization Approach
Author:
Affiliation:
1. Department of Chemistry, University of Natural Resources and Applied Life Sciences Vienna, Muthgasse 18, A-1190 Vienna, Austria, and Graduate School of Agriculture, Kyoto University, Sakyo-ku, Kyoto 606-8502, Japan
Publisher
American Chemical Society (ACS)
Subject
Materials Chemistry,Polymers and Plastics,Biomaterials,Bioengineering
Link
https://pubs.acs.org/doi/pdf/10.1021/bm9006612
Reference13 articles.
1. Synthesis of methyl 4′-O-methyl-13C12-β-d-cellobioside from 13C6-d-glucose. Part 1: Reaction optimization and synthesis
2. Synthesis of methyl 4′-O-methyl-β-d-cellobioside-13C12 from d-glucose-13C6. Part 2: Solid-state NMR studies
3. Synthesis of the perdeuterated cellulose solventsN-methylmorpholineN-oxide (NMMO-d11) andN,N-dimethylacetamide (DMAc-d9)
4. Synthesis of the perdeuterated cellulose solvents N-methylmorpholine N-oxide (NMMO-d11 and NMMO-15N-d11), N,N-dimethylacetamide (DMAc-d9 and DMAc-15N-d9), 1-ethyl-3-methylimidazolium acetate (EMIM-OAc-d14) and 1-butyl-3-methylimidazolium acetate (BMIM-OAc-d18)
5. Synthesis of the perdeuterated cellulose solvents 1-ethyl-3-methylimidazolium acetate (EMIM-OAc-d14) and 1-butyl-3-methylimidazolium acetate (BMIM-OAc-d18) and of 2-13C-butyl-3-methylimidazolium acetate
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