Toward the Creation of NMR Databases in Chiral Solvents: Bidentate Chiral NMR Solvents for Assignment of the Absolute Configuration of Acyclic Secondary Alcohols
Author:
Affiliation:
1. Department of Chemistry and Chemical Biology, Harvard University, 12 Oxford Street, Cambridge, Massachusetts 02138
Publisher
American Chemical Society (ACS)
Subject
Organic Chemistry,Physical and Theoretical Chemistry,Biochemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/ol0171160
Reference5 articles.
1. Compound8aand8bwas prepared by NaBH4reduction of 4-tert-butyl-cis-2-cis-6-dimethylcyclohexanone (Kenar, J. A.; Nickon, A.Tetrahedron1997,53, 14871−14894) and separation by SiO2column chromatography.
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