1. University of Münster, Institute of Physical Chemistry and Sonderforschungsbereich 458, Corrensstrasse 30/36, 48149 Münster, Germany, Max Planck Institute for Solid State Research, Heisenbergstrasse 1, 70569 Stuttgart, Germany, and European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 220, 38043 Grenoble CEDEX, France