Acetylide Participation in Ligand Substitution and P−C Bond Cleavage in the Reaction between HRu3(CO)9(μ3,η2,η2,η1-C⋮CPh) and 4,5-Bis(diphenylphosphino)-4-cyclopenten-1,3-dione (bpcd). Syntheses and X-ray Structures of HRu3(CO)7[μ3,η2,η2,η1,η1,η1-Ph2PCCC(O)CH2C(O)PPh2CCPh] and Ru3(CO)7(μ,η2,η1-PhCCHPh)[μ2,η2,η1- PPhCCC(O)CH2C(O)PPh2]
Author:
Affiliation:
1. Department of Chemistry, University of Houston, Houston, Texas 77204
2. Department of Chemistry, University of North Texas, Denton, Texas 76203
Publisher
American Chemical Society (ACS)
Subject
Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/om0300169
Reference39 articles.
1. Regiospecific substitution of trialkylphosphines for carbon monoxide in hydridoorganoruthenium clusters
2. Chemistry of multisite-round ligands: crystal and molecular structure of HRu3(CO)8(C.tplbond.C-tert-Bu)(PPh2OEt)
3. Bis(disphenylphosphino) acetylene as a bridging ligand between homo- and hetero-metallic clusters
4. Chemistry of multi-site bound unsaturated ligands on metal carbonyl clusters. Intramolecular reductive coupling in the conversion of [Ru3(µ-H)(CO)9(µ3,η2-CCBut)] to the butadienyl cluster [Ru3(CO)8{µ3,η4C(But)CC(H)C(Ph)(PPh2)}], and its crystal structure. An example of ligand isomerism on metal clusters
5. Reactivity of a Triruthenium Acetylide Complex toward Alkynes and the Silica-Mediated Dehydration of Cluster-Bound Alkynols: X-ray Crystal Structures of the Novel Butadienyl Species [Ru3(CO)8{μ3-η8-C(But)CC(Ph)C(H)Ph}] and the Unusual Complex [Ru3(CO)5(μ-CO){μ3-η5-CC(But)- OC(Ph)2CCH}{μ3-η6-CHC(CPh2OH)COC(CPh2)CH}]
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