Surface Organometallic Chemistry: A New Synthesis of [Re2(CO)6(μ-OH)3]- from [Re(CO)3OH]4 Supported on a Silica Surface Added with K2CO3; Evidence of Its Thermal Binding to the Surface via Re−O−Si⋮ Bonds Confirmed by the Synthesis of the Molecular Models [Re2(CO)6(μ-OH)x(μ-OSiEt3)3-x]- (x = 0, 1, or 2) by Reaction of [Re2(CO)6(μ-OH)3]- with Et3SiOH
Author:
Affiliation:
1. Dipartimento di Chimica Inorganica, Metallorganica e Analitica and Centro CNR “CSSSCMTBSO”, Università di Milano, Via G. Venezian, 21, 20133 Milano, Italy
Publisher
American Chemical Society (ACS)
Subject
Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/om010009p
Reference65 articles.
1. Surface Catalytic Sites Prepared from [HRe(CO)5] and [H3Re3(CO)12]: Mononuclear, Trinuclear, and Metallic Rhenium Catalysts Supported on MgO
2. Mononuclear rhenium carbonyls on magnesia: characterization of the metal-support interface by extended x-ray absorption fine structure spectroscopy
3. Rhenium subcarbonyls on magnesium oxide: identification of the surface oxo and hydroxo ligands by infrared spectroscopy
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